TY - JOUR
T1 - Role of hot-pressing temperature on densification and microstructure of ZrB2–SiC ultrahigh temperature ceramics
AU - Nguyen, Van Huy
AU - Delbari, Seyed Ali
AU - Shahedi Asl, Mehdi
AU - Sabahi Namini, Abbas
AU - Ghassemi Kakroudi, Mahdi
AU - Azizian-Kalandaragh, Yashar
AU - Le, Quyet Van
AU - Mohammadi, Mohsen
AU - Shokouhimehr, Mohammadreza
N1 - Publisher Copyright:
© 2020 Elsevier Ltd
PY - 2020/12
Y1 - 2020/12
N2 - This examination is aimed to study the various densification mechanisms in the ZrB2-SiC system at different sintering temperatures. For such an objective, hot-pressing process was implemented to fabricate three ceramics at sintering temperatures of 1650, 1850, and 2050 °C under 10 MPa for 1 h. According to the results, particle rearrangement and fragmentation were the predominant densification mechanisms at the lowest sintering temperature. Additionally, it was found that the activation of the liquid phase sintering mechanism was advantageous in the particle rearrangement at low temperatures. However, rising the sintering temperature to 1850 °C changed the dominant mechanism to the plastic deformation. Such a phenomenon was accompanied by the creation of many dislocations in both ZrB2 and SiC grains. Implementing a higher sintering temperature (2050 °C) activated another consolidation mechanism called diffusion. This occurrence, together with the evaporation of the majority of the liquid phase at elevated temperatures, resulted in emerging transgranular fracture mode in the sample.
AB - This examination is aimed to study the various densification mechanisms in the ZrB2-SiC system at different sintering temperatures. For such an objective, hot-pressing process was implemented to fabricate three ceramics at sintering temperatures of 1650, 1850, and 2050 °C under 10 MPa for 1 h. According to the results, particle rearrangement and fragmentation were the predominant densification mechanisms at the lowest sintering temperature. Additionally, it was found that the activation of the liquid phase sintering mechanism was advantageous in the particle rearrangement at low temperatures. However, rising the sintering temperature to 1850 °C changed the dominant mechanism to the plastic deformation. Such a phenomenon was accompanied by the creation of many dislocations in both ZrB2 and SiC grains. Implementing a higher sintering temperature (2050 °C) activated another consolidation mechanism called diffusion. This occurrence, together with the evaporation of the majority of the liquid phase at elevated temperatures, resulted in emerging transgranular fracture mode in the sample.
KW - Densification
KW - Hot-pressing
KW - Microstructure
KW - SiC
KW - TEM
KW - ZrB
UR - http://www.scopus.com/inward/record.url?scp=85089575137&partnerID=8YFLogxK
U2 - 10.1016/j.ijrmhm.2020.105355
DO - 10.1016/j.ijrmhm.2020.105355
M3 - Article
AN - SCOPUS:85089575137
SN - 0263-4368
VL - 93
JO - International Journal of Refractory Metals and Hard Materials
JF - International Journal of Refractory Metals and Hard Materials
M1 - 105355
ER -