Microstructural, thermal and mechanical characterization of TiB 2 –SiC composites doped with short carbon fibers

Sahar Nekahi, Farhad Sadegh Moghanlou, Mohammad Vajdi, Zohre Ahmadi, Amir Motallebzadeh, Mehdi Shahedi Asl*

*Corresponding author for this work

Research output: Contribution to journalArticlepeer-review

100 Citations (Scopus)

Abstract

Spark plasma sintering method, at the temperature of 1800 °C under the pressure of 40 MPa for 7 min, was employed for fabrication of TiB 2 –SiC-based composites. The influences of short carbon fiber (C f ) addition (2 wt%) on microstructural, mechanical and thermal properties of TiB 2 –SiC ceramics were studied. Carbon fiber addition increased the relative density of sintered composite which observed to have direct effect on mechanical and thermal properties. The mechanical properties of composites were measured by nanoindentation method. Hardness and elastic modulus of TiB 2 /SiC interfaces in carbon fiber doped composite were measured 27.1 GPa and 445 GPa, respectively, while these values were obtained 24.2 GPa and 422 GPa for carbon-free sample. The thermal diffusivity of samples was measured by laser flash technique (LFT). It was found that TiB 2 –SiC–C f composite has a higher thermal conductivity (55 w/m.K) compared to TiB 2 –SiC ceramic with a value of 54.8 w/m.K.

Original languageEnglish
Pages (from-to)129-135
Number of pages7
JournalInternational Journal of Refractory Metals and Hard Materials
Volume82
DOIs
Publication statusPublished - Aug 2019
Externally publishedYes

Keywords

  • Carbon fiber
  • Microstructure
  • Nanoindentation
  • Spark plasma sintering
  • Thermal conductivity
  • TiB –SiC

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